High pressure reactor varioso

Specifications

• Nominal volume ml: 60, 100
• Working volume ml: 20-40, 40-60
• Working pressure bar: 200, 280, 480
• Working temperature °C: 200, 250, 300
• Material WNr. 1.4435 at 200 bar - WNr. 2.4602 at 250 bar - WNr. 1.4980 at 280 bar
• Union nut as lock M48 x1.5 mm, width across flats SW55
• Double sealed: O-ring and medium seal metal to metal (cutting ring).
• Sitec 3-way valve with metering spindle for gas supply and pressure relief
• Pressure gauge in chemical version
• Bursting disc holder equipped with bursting disc
• Immersion tube for thermocouple with ø 3 mm (without thermocouple)
• Temperature sensor Pt1000 or type K suitable

The magnetic stirrer hotplate for highest demands and highest safety

• Heidolph heating plate with magnetic stirrer diameter 145 mm
• Insulating jacket and cooling water connection in the dimensions matched to the heating plate
• The cooling coil for water cooling is mounted on the copper sleeve inside the insulating jacket
• Flow and return have a connection M16 x 1 mm
• Additional borehole for mounting a thermosensor if the jacket temperature is to be regulated
• All-round sealed housing against corrosive gases and liquids
• Protection of the plug connections at the back of the unit
• Strong stirrer magnet for reliable stirring rod entrainment
• Optimum safety due to overheating protection and single magnetic stirrer with 4 safety circuits
• Unintentional adjustment of the set temperature impossible
• Safety shut-off via second independent Pt 100 in the heating plate
• Adjustable safety temperature at which the unit switches off
• Digital display for set and actual temperature, safety T, speed
• Guaranteed not to exceed the selected set temperature (protection of thermolabile substances)
• Electronically controlled speed, control accuracy ±1%.
• RS 232 interface and analogue output MR 3004 safety series

Variants/special features

• Basic model: Central fitting with 3 connections + 1 x reactor cover or 4 connections starting directly from the reactor cover.
• Pressure stages: 200, 250 or 480 bar depending on the choice of material.
• Temperature stages °C: 200, 250, 300 depending on the choice of material.
• Material for wetted parts WNr.: 1.4435 (AISI 316L), 2.4602 (HC22) and 1.4980 (AISI 660) as standard. Versions in Hastelloy C276, B3 or titanium size 2 on request.
• The autoclave vessel is double-sealed: once in the upper area by an O-ring made of Viton, EPDM or Kalrez and at the bottom via a metal-to-metal medium seal (cutting ring).
• Temperature sensor Pt1000, type K or type N in the immersion tube for measuring the medium temperature (not included in delivery).